Curing of fiber-resin mixtures is often the critical and productivity controlling step in the fabrication of thermosetting-matrix composites. The long processing times (and costs) have remained the fundamental impediment to widespread commercialization of composites. Shortening the cure cycle time, while ensuring a complete and uniform cure in the product, is imperative for realizing the goal of affordable materials processing, and forms the focus of this investigation. Toward addressing the affordability challenge, this paper explores the use of conductive carbon mats embedded inside the composite as a means of providing internal volumetric resistance heating during the cure process. The supplemental heating results in temperature and cure uniformity through the cross section, as well as speeds up the cure process. In the context of application to resin transfer molding, systematic experimental and theoretical studies on various resistive heating configurations are presented. Optimum processing strategies are derived based on the cure time and microstructural product quality considerations. [S1087-1357(00)01101-1]

1.
Carrozino
,
S.
,
Levita
,
G.
,
Rolla
,
P.
, and
Tombari
,
E.
,
1990
, “
Calorimetric and Microwave Dielectric Monitoring of Epoxy Resin Cure
,”
Polym. Eng. Sci.
,
30
, pp.
366
373
.
2.
Lee
,
W. I.
, and
Springer
,
G. S.
,
1984
, “
Interaction of Electromagnetic Radiation with Organic Matrix Composites
,”
J. Compos. Mater.
,
18
, pp.
357
386
.
3.
Lee
,
W. I.
, and
Springer
,
G. S.
,
1984
, “
Microwave Curing of Composites
,”
J. Compos. Mater.
,
18
, pp.
387
409
.
4.
Butler, D., and Engel, R. S., 1994, “On the use of Embedded Graphite Patches for Cure in Resin Transfer Molding,” in Proceedings, ICCM-10, Whistler, Canada, pp. 269–275.
5.
Sancaktar
,
E.
,
Weijian
,
E. M.
, and
Yurgartis
,
S. W.
,
1993
, “
Electric Resistive Heat Curing of the Fiber-Matrix Interface in Graphite/Epoxy Composites
,”
ASME J. Mech. Des.
,
115
, pp.
53
60
.
6.
VanDerSchuur, L., and Pitchumani, R., 1997, “A LabVIEW-based Process Control System for Composites Fabrication,” presented at the LabVIEW Virtual Instrumentation Education Conference, MIT, Cambridge, MA, May.
7.
Han
,
C. D.
,
Lee
,
D. S.
, and
Chin
,
H. B.
,
1986
, “
Development of a Mathematical Model for the Pultrusion Process
,”
Polym. Eng. Sci.
,
26
, pp.
393
404
.
8.
Lem
,
K. W.
, and
Han
,
C. D.
,
1983
, “
Chemorheology of Thermosetting Resin
,”
J. Appl. Polym. Sci.
,
28
, pp.
3155
3183
.
9.
Kamal
,
M. R.
, and
Sourour
,
S.
,
1976
, “
DSC of Epoxy Cure: Isothermal Kinetics
,”
Thermochim. Acta
,
14
, pp.
41
59
.
10.
Ning
,
Q.
, and
Chou
,
T.-W.
,
1995
, “
A Closed-Form Solution of the Transverse Effective Thermal Conductivity of Woven Fabric Composites
,”
J. Compos. Mater.
,
29
, pp.
2280
2294
.
11.
Condon, E. U., and Odishaw, H., 1967, Handbook of Physics, McGraw-Hill, New York.
12.
Pitchumani
,
R.
,
Liaw
,
P. K.
,
Yao
,
S. C.
,
Jeong
,
H.
, and
Hsu
,
D. K.
,
1995
, “
Theoretical Models for the Anisotropic Conductivities of Two-Phase and Three-Phase Metal-Matrix Composites
,”
Acta Metall. Mater.
,
43
, pp.
3045
3059
.
13.
Incopera, F. P., and DeWitt, D. P., 1996, Fundamentals of Heat and Mass Transfer, Wiley, New York.
14.
Rai
,
N.
, and
Pitchumani
,
R.
,
1997
, “
Optimal Cure Cycles for the Fabrication of Thermosetting-matrix Composites
,”
Polym. Compos.
,
18
, pp.
556
581
.
15.
Russ, J. C., 1995, The Image Processing Handbook, CRC, Boca Raton, FL.
16.
Zhu
,
L.
, and
Pitchumani
,
R.
,
1999
, “
Processing Envelopes for Supplemental Internal Resistive Heating during Thermosetting-Matrix Composite Cure
,”
J. Reinf. Plast. Compos.
,
18
, No.
13
, pp.
1242
1253
.
17.
Zhu, L., and Pitchumani, R., 1999, “Analysis and Design of a Thermosetting Matrix Cure Process with Supplemental Internal Resistive Heating,” Compos. Sci. Technol., submitted.
You do not currently have access to this content.